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differential mass spectrometry hpr-40  (Hiden Analytical)
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Hiden Analytical differential mass spectrometry hpr-40
a) Galvanostatic profile of Li 6 CoO 4 during charge to 4.3V vs. Li/Li + and changes in half‐height position at different state of charge obtained from X‐ray absorption near edge <t>spectroscopy</t> of Co K‐edge. b) X‐ray absorption near edge spectroscopy (XANES) of Co K‐edge at different state of charge. c) in situ XRD contour maps of (101) and (201) diffraction peaks that indicates anti‐fluorite structure. d) O 2 and CO 2 evolution measured by OEMS quantitative in situ analysis.
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a) Galvanostatic profile of Li 6 CoO 4 during charge to 4.3V vs. Li/Li + and changes in half‐height position at different state of charge obtained from X‐ray absorption near edge spectroscopy of Co K‐edge. b) X‐ray absorption near edge spectroscopy (XANES) of Co K‐edge at different state of charge. c) in situ XRD contour maps of (101) and (201) diffraction peaks that indicates anti‐fluorite structure. d) O 2 and CO 2 evolution measured by OEMS quantitative in situ analysis.

Journal: Advanced Science

Article Title: Gas Evolution Kinetics in Overlithiated Positive Electrodes and its Impact on Electrode Design

doi: 10.1002/advs.202400568

Figure Lengend Snippet: a) Galvanostatic profile of Li 6 CoO 4 during charge to 4.3V vs. Li/Li + and changes in half‐height position at different state of charge obtained from X‐ray absorption near edge spectroscopy of Co K‐edge. b) X‐ray absorption near edge spectroscopy (XANES) of Co K‐edge at different state of charge. c) in situ XRD contour maps of (101) and (201) diffraction peaks that indicates anti‐fluorite structure. d) O 2 and CO 2 evolution measured by OEMS quantitative in situ analysis.

Article Snippet: Online differential mass spectrometry (HPR‐40, Hiden Analytical) was modified to accommodate gas analysis on Li‐ion batteries.

Techniques: Spectroscopy, In Situ